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Metallography Examples

Powder metal fracture SEM micrograph
Powder metal SEM image

The Scanning Electron Microscope (SEM) image to the right was prepared as part of the failure analysis of a powder metal part that failed in service. The image was part of the analysis to answer the questions:

The questions were answered by a combinations of this image, optical microscopy and process detective work (including talking with production operators).

52100 TEM micrograph
TEM replica of AISI 52100 - 12,500x original magnification

The Transmission Electron Microscope (TEM) image to the right is from my associate's files. It is a cross section of a AISI 52100 steel miniature ball bearing inner race.

Failures during gyroscope testing stopped production for the the Apollo Lunar Landing and a Navy ballistic missile programs. The production halt jeapordized both lunar landings and fleet readiness.

All the solutions proposed by the bearing manufacturers (New Departure and Barden), and other experts, were tried - without success. One next step was using the best available technology to look deeper into the microstructure of old (good) and new (bad) bearings.

The image was taken in 1968. At the time, the only option beyond optical microscopy magnification was using TEM replicas. TEM images required polishing the sample, depositing a layer of chrome on the surface, removing the chrome layer (the replica) and imaging the replica in the electron microscope.

This, and other, TEM images were taken to determine differences in bearing steel microstructures among:

No metallurgical differences were found that explained the differences in factory yield and field performance. While TEM did not provide the "solution," it was very valuable because the TEM results closed the door to "blaming" the metal.

My associate subsequently identified a change to the assembly and test system that was put into production. The changes increased service life for both new bearings by more than 5x and solved production yield issues.

Thermal Etch
Thermal Etch Micrograph

This image of the cross section of a titanium sheet explosive welded to a tantalum sheet is a higher magnification of one of the welded layers of the image on the home page.

The picture illustrates the intense cold working done by the shock wave from the explosive detonation as the shock wave traveled across the plates to be welded together.

There is no evidence of intermetallic compound formation from the welding process.

Site Updated January 7, 2018 rev 10